IS 16658 : 2018 Tobacco and Tobacco Products - Cigarette Filters - Determination of Nicotine Alkaloid Retention Index and Water Retention Index by Gas Chromatography - Direct Method

ICS 65.160

FAD 04

Reaffirmed 2023

1. SCOPE

1.1 This standard prescribes a direct method for the determination of nicotine alkaloid retention index and water retention index of cigarette filters by gas - chromatographic analysis.

1.2 The method is applicable to filter cigarettes. This method shall be used unless it is not applicable owing to incomplete recovery of the retained nicotine alkaloid from the filter material (for example, with some types of charcoal filters). In case of tip ventilated cigarettes, the ventilation shall be completely blocked by a suitable self adhesive tape.

2. REFERENCES

The standards listed below contain provisions which, through reference in this text, constitute provisions of this standard. At the time of publication, the editions indicated were valid. All standards are subject to revision and parties to agreements based on this standard are encouraged to investigate the possibility of applying the most recent editions of these standards indicated below: 1070 : 1992 Reagent grade water - Specification (third revision) 12942 : 2008/ISO 8243 : 2006 Cigarettes - Sampling (second revision) 16022 : 2012/ISO 3308 : 2012 Routine analytical cigarette - Smoking machine - Definitions and standard conditions 16023 : 2012/ISO 4387 : 2000 Cigarettes - Determination of total and nicotine-free dry particulate matter using a routine analytical smoking machine 16025 : 2012/ISO 10315 : 2013 Cigarettes - Determination of nicotine in smoke condensates - Gas chromatographic method 16042 : Part 1 : 2012/ISO 10362-1 : 1999 Cigarettes - Determination of water in smoke condensates: Part 1 Gas-chromatographic method 16121 : 2013/ISO 3402 : 1999 Tobacco and tobacco products - Atmosphere for conditioning and testing 16133 : 2018 Cigarettes - Determination of alkaloid retention by the filters Spectrometric method